This review provided a detailed overview of the different synthesis and characterization methods of polymeric nanoparticles. Nanoparticles are defined as solid and colloidal particles of macromolecular substances ranging in size under 100 nm. Different types of nanoparticles are used in many biological fields (bio-sensing, biological separation, molecular imaging, anticancer therapy, etc.). The new features and functions provided by nano dimensions are largely different from their bulk forms. High volume/surface ratio, improved resolution and multifunctional capability make these materials gain many new features.
The cambucizeiro (Campomanesia phaea), belonging to the Myrtaceae family, is a native plant of the Brazilian Atlantic Forest. The description of the characteristics of the cambucizeiro fruits is important to support new genetic improvement works and its commercial exploitation, especially regarding the processing of the fruit. The present work aimed to perform the morphological and chemical characterization of the cambucizeiro fruits. Fifty-eight accessions, from different locations in the Atlantic Forest and Serra do Mar in the state of São Paulo, were collected, propagated by seeds and one specimen of each accessory is at the Seedling Production Center in São Bento do Sapucaí (SP). Forty fruits from each access were collected in May and submitted to the following analyses: longitudinal and transversal diameter, total fruit fresh mass, number and mass of seeds, total soluble solids, % citric acid, ratio, firmness, vitamin C and coloration. Fruit conformation varies intensely among accessions. The number of seeds is not a good indicator for the relation with the fruit mass, but the mass of one thousand seeds. Some accessions have high soluble solids content, but, on the other hand, the vast majority have fruits with high acidity. Cambuci is an excellent source of vitamin C. The fruits of the accessions are green in color, persisting an opaque shade when ripe.
Our environment has been significantly impacted by man-made pollutants, primarily due to industries making substantial use of synthetic chemicals, resulting in significant environmental consequences. In this research investigation, the co-precipitation approach was employed for the synthesis of cellulose-based ferric oxide (Fe2O3/cellulose) and copper oxide nanoparticles (CuOx-NPs). Scanning electron microscopy (SEM) analyses were conducted to determine the properties of the newly synthesised nanoparticles. Furthermore, the synthesized nanoparticles were employed for eliminating chromium from aqueous media under various conditions, including temperature, contact time, adsorbent concentration, adsorbate concentration, and pH. Additionally, the synthesised materials were used to recover Cr(VI) ions from real samples, including tap water, seawater, and industrial water, and the adsorptive capacity of both materials was evaluated under optimal conditions. The synthesis of Fe2O3/cellulose and CuOx-NPs proved to be effective, as indicated by the outcomes of the study.
Magnetic graphene oxide nanocomposites (M-GO) were successfully synthesized by partial reduction co-precipitation method and used for removal of Sr(II) and Cs(I) ions from aqueous solutions. The structures and properties of the M-GO was investigated by X-ray diffraction, Fourier transformed infrared spectroscopy, X-ray photoelectron spectroscopy, transmission electron microscopy, scanning electron microscopy, vibrating sample magnetometer (VSM) and N2-BET measurements. It is found that M-GO has 2.103 mg/g and 142.070 mg/g adsorption capacities for Sr(II) and Cs(I) ions, respectively. The adsorption isotherm matches well with the Freundlich for Sr(II) and Dubinin–Radushkevich model for Cs(I) and kinetic analysis suggests that the adsorption process is pseudo-second-ordered.
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