Magnesium hydroxide/melamine phosphate borate (nano MH/MPB), a novel nano-composition intumescent flame retardant, was synthesized with the in-situ reaction method from MgCl2·6H2O sodium hydroxide (NaOH) and melamine phosphate borate (MPB) in the absence of H2O. The structure of the product was confirmed by EDAX IR and XRD. The effects of reaction temperature and time on the dimension of magnesium hydroxide were observed. The effects of mass ratio of magnesium hydroxide to MPB on the flame retardancy of nano-MH/MPB/EP were examined with the limiting oxygen test. The results show that the optimal condition of synthesis of MH/MPB is mMH/mMPB = 0.25, reacting under 75 ℃ for 30 minutes. Finally, the mechanism for flame retardancy of nano-MH/MPB/EP was pilot studied by means of IR of char layer and TG of MH/MPB.
This article describes a classification tool to cluster SARAL/AltiKa waveforms. The tool was made using Python scripts. Radar altimetry systems (e.g., SARAL/AltiKa) measures the distance from the satellite centre to a target surface by calculating the satellite-to-surface round-trip time of a radar pulse. An altimeter waveform represents the energy reflected by the earth’s surface to the satellite antenna with respect to time. The tool clusters the altimetric waveforms data into desired groups. For the clustering, we used evolutionary minimize indexing function (EMIF) with k-means cluster mechanism. The idea was to develop a simple interface which takes the altimetry waveforms data from a folder as inputs and provides single value (using EMIF algorithm) for each waveform. These values are further used for clustering. This is a simple light weighted tool and user can easily interact with it.
In the current work, it was investigated to the K X-ray fluorescence efficiency and chemical effect on vacancy transfer probability for some tin compounds. We used Br2Tin, TinI2, SeTin, TinF2, TinSO4, TinCl2, TinO and TinS compounds for experimental study. The target samples were irradiated with 241Am annular radioactive source at the intensity of 5 Ci which emits gamma rays at wavelength of 0.2028 nm. The characteristic x-rays emitted because of the excitation are collected by a high-resolution HPGe semiconductor detector. It has been determined that the experimental calculations of the tin (Sn) element are compatible with the theoretical calculation. In addition, we have calculated the experimental intensity ratios, fluorescence yields and total vacancy transfer probabilitiesfor other Sn compounds.
Nanotransformations of a blanket at the fair dimensional combined processing with imposing of electric field the tool in the form of untied metal granules are considered. An object of researches are the figurine details applied in aviation, the missile and space equipment and in the oil and gas industry: driving wheels and a flowing part of cases of turbo-pump units, screws, krylchatka where there are sites of variable curvature with limited access of the tool in a processing zone.It is shown that the combination in the combined process of two-component technological environments of current carrying granules and the electroconductive liquid environment given with a high speed to a processing zone allows to receive the required quality of a blanket; action of electric field from a source with the increased tension allows to create at fair dimensional processingthe required peening from blows of firm granules. It gives the chance to raise a resource and durability of responsible knots of the aerospace equipment and oil and gas equipment, to expand the field of use of the combined processing with untied granules on a detailwith the sitesnot available to processing by a profile electrode.
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